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Factory Export Top Purity CYCLOHEPTYL CHLORIDE 2453-46-5 In Stock
- Molecular Formula:C7H13 Cl
- Molecular Weight:132.633
- Vapor Pressure:1.45mmHg at 25°C
- Refractive Index:1.4730-1.4770
- Boiling Point:176.8°Cat760mmHg
- Flash Point:47.9°C
- Density:0.96g/cm3
CYCLOHEPTYL CHLORIDE(Cas 2453-46-5) Usage
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Synthesis Reference(s) |
Journal of the American Chemical Society, 115, p. 3071, 1993 DOI: 10.1021/ja00061a005 |
InChI:InChI=1/C7H13Cl/c8-7-5-3-1-2-4-6-7/h7H,1-6H2
2453-46-5 Relevant articles
Highly selective halogenation of unactivated C(sp3)-H with NaX under co-catalysis of visible light and Ag@AgX
Liu, Shouxin,Zhang, Qi,Tian, Xia,Fan, Shiming,Huang, Jing,Whiting, Andrew
, p. 4729 - 4737 (2018/10/23)
The direct selective halogenation of una...
A alkane halogenation method (by machine translation)
-
Paragraph 0044; 0045, (2017/07/21)
The invention relates to a cycloalkane o...
Photoinduced, Copper-Catalyzed Carbon-Carbon Bond Formation with Alkyl Electrophiles: Cyanation of Unactivated Secondary Alkyl Chlorides at Room Temperature
Ratani, Tanvi S.,Bachman, Shoshana,Fu, Gregory C.,Peters, Jonas C.
supporting information, p. 13902 - 13907 (2016/01/15)
We have recently reported that, in the p...
A facile and green protocol for nucleophilic substitution reactions of sulfonate esters by recyclable ionic liquids [bmim][X]
Liu, Yajun,Xu, Yongnan,Jung, Sun Ho,Chae, Junghyun
, p. 2692 - 2698,7 (2012/12/12)
Ionic liquids [bmim][X] (X = Cl, Br, I, ...
2453-46-5 Process route
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-
291-64-5
cycloheptane
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-
2453-46-5
cycloheptyl chloride
| Conditions | Yield |
|---|---|
|
With
hydrogenchloride; tetrabutyl-ammonium chloride; sodium chloride;
In
water;
at 20 ℃;
for 7h;
|
93% |
|
With
hydrogenchloride; potassium chloride; tetrabutyl-ammonium chloride;
In
water;
at 20 ℃;
Irradiation;
Green chemistry;
|
90% |
-
-
502-41-0
cycloheptanol
-
-
2453-46-5
cycloheptyl chloride
| Conditions | Yield |
|---|---|
|
With
hydrogenchloride;
|
|
|
With
phosphorus pentachloride;
|
|
|
With
boron trichloride;
|
|
|
With
tri-chlorocyanuric acid; triphenylphosphine;
In
acetonitrile;
at 60 ℃;
for 2h;
|
|
|
Multi-step reaction with 2 steps
1: pyridine / 20 °C
2: 1-butyl-3-methylimidazolium chloride / 8 h / 60 °C / Inert atmosphere; Green chemistry
With
pyridine; 1-butyl-3-methylimidazolium chloride;
|
|
|
With
N-chloro-succinimide; triphenylphosphine;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
|
2453-46-5 Upstream products
-
128-09-6
N-chloro-succinimide
-
291-64-5
cycloheptane
-
502-41-0
cycloheptanol
-
628-92-2
Cycloheptene
2453-46-5 Downstream products
-
4277-29-6
cycloheptanecarboxaldehyde
-
16624-02-5
Dimethyl-cycloheptyl-carbinol
-
128217-21-0
trimethyl<(1-methyl-(3-(oxocyclohex-3-yl)-2-propenyl)pentyl)oxy>silane
-
628-92-2
Cycloheptene
